DATA: amount of product collected = 1.727 g boiling range: 130–135 ° QUESTIONS Was the reaction…

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DATA: amount of product collected = 1.727 g boiling range: 130–135 ° QUESTIONS Was the reaction…

DATA:

  • amount of product collected = 1.727 g
  • boiling range: 130–135 °

QUESTIONS

  1. Was the reaction successful? What was the actual yield? (You may need to do some unit conversions for this)
  2. Comment on the boiling range. Can boiling range alone be used to confirm the identity of the product?
  3. Does the IR spectrum show expected signals for the ester? Point to specific stretches that are present in the product but not in the reactants.

Please answer and explain!

%Transmittance 4000 1001 3500 3000 2958.30 2872.14 2500 Wavenumbers (cm-1) 2000 1739.12 1500 1465.49 1387 20 1366.34 1227.62 1171.02 1000 1055.05 1028.86 960.98 818.10 635.04 606.08 500 Dite: 10/24/1 Page 79
00 000C 2958.30 2872.14 2500 Waverumbers (cm-1) 2000 1739.12 1500 1465.49 1387.20 1366.34 122762 1171.02 1000 1055 05 1028.86 960.98 818.10 635 04 606 08 500 Wh/T, 710 be abad
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