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DATA: amount of product collected = 1.727 g boiling range: 130–135 ° QUESTIONS Was the reaction…
DATA:
- amount of product collected = 1.727 g
- boiling range: 130–135 °
QUESTIONS
- Was the reaction successful? What was the actual yield? (You may need to do some unit conversions for this)
- Comment on the boiling range. Can boiling range alone be used to confirm the identity of the product?
- Does the IR spectrum show expected signals for the ester? Point to specific stretches that are present in the product but not in the reactants.
Please answer and explain!
%Transmittance 4000 1001 3500 3000 2958.30 2872.14 2500 Wavenumbers (cm-1) 2000 1739.12 1500 1465.49 1387 20 1366.34 1227.62 1171.02 1000 1055.05 1028.86 960.98 818.10 635.04 606.08 500 Dite: 10/24/1 Page 79
00 000C 2958.30 2872.14 2500 Waverumbers (cm-1) 2000 1739.12 1500 1465.49 1387.20 1366.34 122762 1171.02 1000 1055 05 1028.86 960.98 818.10 635 04 606 08 500 Wh/T, 710 be abad
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